| Parameter | Score |
|---|---|
| 1. Scale | A |
| 2. Study Population | A |
| 3. Samples | A |
| 4. Measurand | A |
| 5. Pre-Analytical | A |
| 6. Replicate Analysis | B |
| 7. Steady State | C |
| 8. Outlier Analysis | C |
| 9. Normality | A |
| 10. Variance Homogeneity | C |
| 11. ANOVA | A |
| 12. CI | A |
| 13. No of Results | C |
| 14. Concentrations | B |
| 15. Total Score | C7,8,10,13 |
| Comment |
| Parameter | Score |
|---|---|
| Matrix | Urine |
| Measurand | Vanillylmandelic acid (VMA) |
| Unit | mg / Unknown |
| Overall Analytical Principle Method | Chromatography; HPLC |
| Number of Subjects | 44 |
| Number of Subjects included in BV estimation | 44 |
| Ethinicity | Caucasian |
| Age Mean / Median | 26.6 |
| Age Min | 25.0 |
| Age Max | 35.0 |
| Age SD | |
| Number of Males | 44 |
| Number of Females | |
| State of Well Being |
Healthy (excl pregnant)
|
| Diseases | |
| Study Duration Length | 2 |
| Study Duration Units | Day |
| Sampling Intervals, e.g. X sample(s) per Interval Unit | 1 |
| Interval Units | Day |
| Sampling Times | Start Time:
20:00
End Time: 7:00 |
| Number of Samples | 2 |
| Average Number of Samples Used for BV Estimation | 2.0 |
| Average Number of Replicates | 0.0 |
| Estimates of CVi | 30.7 |
| Calculated Confidence Intervals of CVi | Lower: 25.39, Upper: 38.84 |
| Estimates of CVg | 64.3 |
| Calculated Confidence Intervals of CVg | Lower: 51.58, Upper: 82.96 |
| Analytical CV | 3.0 |
| Calculated Confidence Intervals of Analytical CV | Lower: 2.03, Upper: 5.75 |
| Measurand Mean | |
| Measurand Min | |
| Measurand Max | |
| Measurand SD |